1.1 ,These test methods cover the chemical analysis of sulfonated and sulfated oils. The analytical procedures appear in the following order:
, | Section |
, | , |
Moisture: | , |
,Test Method A. Water by Distillation with Volatile Solvent | 4 –, 9 |
,Test Method B. Moisture and Volatile Matter by Hot-Plate Method | 10 –, 14 |
Organically Combined Sulfuric Anhydride: | , |
,Test Method A. Titration Test | 15 –, 19 |
,Test Method B. Extraction-Titration Test | 20 –, 24 |
,Test Method C. Ash-Gravimetric Test (in the Presence of True | 25 –, 28 |
Total Desulfated Fatty Matter | 29 –, 32 |
Total Active Ingredients | 33 –, 36 |
Unsaponifiable Nonvolatile Matter | 37 –, 41 |
Inorganic Salts | 42 –, 46 |
Total Alkalinity | 47 –, 49 |
Total Ammonia | 50 –, 52 |
Acidity as Free Fatty Acids or Acid Number: | , |
,Test Method A. In the Absence of Ammonium or Triethanolamine Soaps | 53 –, 56 |
,Test Method B. In the Presence of Dark Colored Oils but in the | 57 –, 60 |
,Test Method C. In the Presence of Ammonium or Triethanolamine Soaps | 61 –, 63 |
Water-Immiscible Organic Solvents Volatile with Steam | 64 –, 70 |